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Results GC-MS peaks identification in hookah tobacco products Volatiles collection using SPME led to the identification of 114 volatile components (Supplementary Table S1) belonging to 13 major classes of volatile compounds comprising esters, oxygenated monoterpenes, ketones, alcohols, lactones, aldehydes/furans, nitrogenous compounds/alkaloids, aromatics, acetals, phenols, monoterpene hydrocarbons, acids, and sesquiterpene hydrocarbons (Figs 2 and 3)