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Mobile phase A consisted of 10 mM ammonium acetate in water (pH 9) with a 5 M Agilent InfinityLab deactivator additive (p/n 5191-4506), and mobile phase B consisted of 10 mM ammonium acetate (pH 9) in 10:90 (v:v) water/acetonitrile with a 5 M Agilent InfinityLab deactivator additive (p/n 5191-4506)

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