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10.1016/j.expneurol.2013.08.019 94 LippmannE

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Alloc in the Fmoc-Lys(Alloc)-OH in the preparation method is removed twice with 5-10 equivalents of morpholine (or 5-10 equivalents of phenylsilane as an alternative thereof) and 0.1-0.3 equivalents of Pd(PPh 3 ) 4 for 10-30 min each time, wherein CH 2 Cl 2 is used as a solvent in the removal