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Upon addition of ME, the olefinic proton (H a ) of TPE-DCV with chemical shift of ~8.4 ppm disappears and a new peak (H b ) at 4.69 ppm arises, suggestive of the addition reaction of thiol on the vinyl group (Figure S6) 58

In humans, a RCT enrolling 156 patients with a BMI 27 kg/m 2 failed to demonstrate that one year of liraglutide treatment could improve pain in patients with KOA compared to placebo, despite a significant BW difference of approximately 4 kg at end of study 105

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