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M.ThorburnD

doi: 10.1038/s41593-018-0231-0 74 KalinowskaMvan der LeiMBKitiashviliMMamcarzMOliveiraMMLongoFet al

Gastroenterology (2017) 152:73044

Briefly, the resin was swollen in DMF for 1 h and, subsequently, the Fmoc protecting group was cleaved with a piperidine solution (20 vol% in DMF) by microwaving at 155 W, 75 C for 15 s and at 30 W, 90 C for 50 s