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No activities on the bile duct were performed on five patients
1 H NMR (500 MHz, CDCl 3 ) 8.037.98 (m, 1H), 7.867.81 (m, 1H), 7.667.60 (m, 2H), 7.437.36 (m, 4H), 6.96 (d, J = 16.0 Hz, 1H), 6.86 (d, J = 16.0 Hz, 1H), 6.80 (s, 1H), 3.16 (s, 2H), 2.58 (s, 2H), 2.43 (s, 2H), 2.33 (s, 3H), 1.59 (s, 6H), 1.06 (s, 6H) ppm
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