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Sadly, the expiry was the end of April 2021, so perhaps they're too far gone now

Once it neutralizes a free radical, it gets used up and needs to be recycled back into its active state

Through cleavage of dynamic phenylboronic ester bonds under ROS stimulation 62 , the hydrogel demonstrated ROS-sensitive drug release behavior, as evidenced by the 90% cumulative release of D-CuP within 72 h under H 2 O 2 stimulation (Fig